New Terahertz Material Characterization System Installed in Brown University Lab

Unique CW-THz spectroscopy system to aid Mittleman Lab in materials research.

Brown University scientists exploring how frequencies within the terahertz band of the electromagnetic spectrum can advance spectroscopic studies of materials recently added a new tool to their research arsenal: a THz-frequency materials characterization system from Lake Shore Cryotronics.

Installed in the lab of Professor Dan Mittleman in early March by Lake Shore, the 8500 Series system will be used primarily to study THz-frequency magneto-optical responses of semimetals, iron-based superconductors and other novel materials.

Dr. Mittleman’s research interests involve the science and technology of terahertz radiation. He moved last year from Rice University to Brown to start up the world-class THz research facility in the university’s School of Engineering. Since his arrival in September, the Mittleman Lab has assembled an impressive array of equipment and staff to continue explorations in the THz regime, commonly considered “the last frontier” of the electromagnetic spectrum.

Researchers have long believed that THz analysis could reveal new and important properties of materials, and open new doors to further semiconductor and materials development. However, there was a need for affordable, reliable and easily operable measurement systems for the research community.

The 8500 Series system from Lake Shore represents the first commercially available product to combine continuous wave (CW) THz spectroscopy and a high-field cryostat to create a reliable tool for researching the far infrared properties of new materials. No special knowledge of THz optics is required, and it enables non-contact material spectroscopic response measurements across a wide range of frequencies, temperatures and field strengths.

Unlike conventional pulsed THz spectroscopy techniques, the Lake Shore system uses a tunable source of THz frequency energy to enable high-resolution spectroscopic studies of the magneto-optic properties of materials, in conjunction with specially developed, cryogenically stable THz emitter and detector devices.

Lake Shore partnered with TOPTICA Photonics AG of Munich, Germany to adapt that company’s proven CW-THz spectrometer product for this ground-breaking system integration application.

According to Dr. David Daughton, the Lake Shore applications scientist who led the team of hardware and software developers to create the 8500 Series system, TOPTICA’s experience in research-grade lasers and laser controllers proved critical to achieving the rock-solid measurement performance required in this very demanding application.  

We set out to accomplish something never done before – placing a CW-THz measurement inside a research cryostat so that samples can be analyzed spectroscopically at temperatures as low as 5 Kelvin.

It turns out this is a lot harder than it sounds because THz signals are very small, and everything has to be very stable and repeatable for the measurements to be meaningful. Slight variations in temperature, THz source power or background signals can be detrimental. It took a lot of work to sort it all out, but we are pleased with the final product and look forward to the research results it will enable.

Dr. David Daughton - Applications Scientist, Lake Shore

The delivery of its first production THz system to Brown was the culmination of more than four years of product development, beta site testing and refinement by Lake Shore and its partner institutions. Beginning in late 2011, Lake Shore worked closely with researchers at The Ohio State University, the University of Dayton, Wright State University, the University of Arizona, and the Air Force Research Lab to refine product concepts and perform early testing in a variety of material measurement applications.

Lake Shore believes the 8500 Series system will also provide new insights in many emerging electronic, magnetic and chemical material research applications, including photovoltaics, organic electronics, and spin-based computing studies where scientists can use spectroscopic response measurements to derive key material properties. These include dielectric constant, dynamic conductivity, carrier scattering mobilities and vibrational and magnetic resonances.

Mittleman’s group will continue to spearhead research into new techniques for generating, manipulating and detecting terahertz radiation, with a goal of eventually opening a user facility to further support others working in this arena.

For more information about the 8500 Series system, click here.


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