iSorbHP High Pressure Volumetric Apparatus

The iSorb HP gas-sorption analyzers are ideal for assessing materials used in gas storage, gas separation, or emission control applications.

Featuring high-accuracy transducers, accurate manifold temperature regulation, and an integrated library of advanced equations of state, the iSorb HP line provides access to reliable gas adsorption and kinetic data up to 100 bar or 200 bar absolute.

Optional temperature-control accessories enable measurements over a temperature range of 75 K to 773 K.

HP1 100

  • Single-station sorption analyzer
  • High-pressure testing up to 100 bar pressure

HP1 200

  • One-station gas sorption analyzer
  • High-pressure testing up to 200 bar pressure

HP2 100

  • Two-station gas sorption analyzer
  • High-pressure measurements up to 100 bar pressure

HP2 200

  • High-pressure testing up to 200 bar pressure
  • Two-station gas sorption analyzer

Key Features

Robust Manifold Design Ensures Results are Not Affected by Temperature and Ambient Conditions

High-pressure testing requires a controlled temperature to achieve accurate, precise results. As such, the iSorb HP manifold is thermostatically warmed above ambient temperature to improve stability and shield from environmental variations.

Microprocessor-driven digital pressure transducers deliver temperature-compensated pressure measurements. The software monitors the stability of the manifold temperature and gas pressure before dosing into the sample cell; readings taken at steady temperatures yield the most accurate and precise measurements possible. Metal VCR seals and pneumatic valves guarantee leak-tight operation.

Two women look at the work flow of high-pressure experiments and temperature control.

Image Credit: Anton Paar GmbH 

Highly Flexible Experimental Conditions

iSorb HP offers a selection of high pressure sample cells designed to support a broad range of sample forms: powders, granules, films, and monoliths. Sample temperature is regulated using multiple accessories ranging from cryogenic (75 K) to high temperatures (773 K).

The low-volume microcell allows the user to evaluate material performance even when the sample quantity is limited. Reduced void space, combined with precise temperature control, eliminates the need for blank-subtraction runs.

The compact pressure booster delivers a 4:1 compression output, sustaining 200 bar with only 55 bar remaining in the gas cylinder to save money and resources.

iSorbHP High Pressure Volumetric Apparatus equipment photo.

Image Credit: Anton Paar GmbH 

Peace of Mind with Built-In Safety

Operating at elevated pressures with hazardous gases makes safety a top priority. With the iSorb HP, sample cell pressure is continuously tracked, even during a power failure; in the event of a power outage, the instrument automatically shuts all valves. Its “Safe State” routine restores the manifold and sample cell to ambient pressure using helium, allowing easy sample removal.

The intelligent software includes an automatic leak-detection algorithm that can distinguish between adsorption and a leak. If a leak is identified, the instrument halts the analysis, returns to a safe state, and can activate an external alarm. An automated supply-line cleaning routine prevents the mixing of incompatible gases.

iSorbHP High Pressure Volumetric Apparatus

Image Credit: Anton Paar GmbH 

Insights into Sample Kinetics, Heat Adsorption at Different Temperatures, and More

Surface excess isotherms can be readily generated using the iSorb HP through two integrated approaches: traditional target-pressure mode or quicker pressure dosing.

Users may also examine sample kinetics for every data point acquired and compute the heat of adsorption from several isotherms measured at varying analysis temperatures. Absolute adsorbed amount isotherm and storage capacity calculations support R&D in identifying future innovative materials for gas storage capabilities.

iSorbHP High Pressure Volumetric Apparatus a desktop showing the screen format of the iSorb HP computer program.

Image Credit: Anton Paar GmbH 

Permanent Control of Instrument Status and Health

The valve management system tracks every valve cycle to assist in planning maintenance schedules. The exportable visual log file captures all pressure and temperature data, valve actions, and animated graphics for quick diagnostics and full analysis playback.

A man in plain clothes and a woman wearing a lab coat look at the pressure output from a spectrum.

Image Credit: Anton Paar GmbH 

Specifications

Source: Anton Paar GmbH 

Performance/physical iSorb HP1 iSorb HP2
Analysis stations 1 2
Gas inputs 2 (optional 4)
Maximum pressure data 100 bar or 200 bar absolute
Minimum pressure data 0.0005 bar
Low Pressure (LP) transducers 2 (1 bar) 3 (1 bar)
High Pressure (HP) transducers 2 3
Total transducer count 4 6
Transducer accuracy <±0.05 % f.s
Vacuum pump internal
Turbo pump option yes
Degas type automatic
Degas ports in-situ
Max. degas temp 500 °C
Thermostatted bath option yes
Cryo option yes
Booster option yes
Thermostatted manifold yes
Gas inputs/vents location Side, for easy access
Dimensions (W × H × D) 85 cm × 100 cm × 50.5 cm (33.5 in × 39.25 in × 19.5 in)
Weight 150 kg (330 lbs) 150 kg (330 lbs)

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